Macedonite, PbTiO3, occurs as tiny grains and crystals in the amazonite quartz syenite veins in Crni Kamen near Prilep, Macedonia, Yugoslavia. It is tetragonal: a, 3.889 ± 0.024 Å; c 4.209 ± 0.036 Å. The strongest X-ray powder diffraction lines are (Å): 2.843 (10), 2.728 (8), 2.284 (7), 1.954 (7), and 1.603 (9). Specific gravity is 7.82 Å 0.06. Microhardness is 507 Å 30 kg/mm2 which corresponds to 5.5 on the Moh scale. Macedonite is soluble in warm HCl, HNOs, and H2SO4. Chemical analysis: PbO 70.55%, Bi2O3 2.20%, TiO2 25.07%, and FeO 2.69%. Macedonite is geneticaly related to the differentiation of an alkali syenitic magma and has been formed in the pegmatitic-pneumatolytic stage as an accessory mineral.

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