Abstract This paper shows how heavy minerals and single-grain varietal studies can be conducted on silt (representing c. 50% of world's sediments) sediments to obtain quantitative data as efficiently as for sand-sized sediments. The analytical workflows include heavy mineral separation using a wide grain-size window (15–355 μ) analysed through integrated optical analysis, Raman spectroscopy, QEMSCAN microscopy and U–Pb dating of detrital zircon. Upper Jurassic–Cretaceous silt-sized sediments from the Mandawa Basin of central-southern Tanzania have been selected for the scope of this research. Raman-aided heavy mineral analysis reveals garnet and apatite to be the most common minerals together with durable zircon, tourmaline and subordinate rutile. Accessory but diagnostic phases are titanite, staurolite, epidote and monazite. Etch pits on garnet and cockscomb features on staurolite document the significant effect of diagenesis on the pristine heavy mineral assemblage. Multivariate statistical analysis highlights a close association among durable minerals (zircon, tourmaline and rutile, ZTR) while garnet and apatite plot alone reflecting independence between the three groups of variables with garnet increasing in Jurassic samples. Raman data for garnet end-member analysis document different associations between Jurassic (richer in A, Bi and Bii types) and Cretaceous (dominant A, Ci and Cii types) samples. U–Pb dating of detrital zircon and their statistical integration with the above-mentioned datasets provide further insights into changes in provenance and/or drainage systems. Metamorphic rocks of the early and late Pan-African orogeny terranes of the Mozambique Belt and those of the Irumide Belt acted as main source of sediment during the Jurassic. Cretaceous sediments record a broadening of the drainage system reaching as far as the Usagran–Ubendian Belt and the Tanzanian Archean Craton.

ABSTRACT We measured stratigraphic sections and collected samples from Oceanic suite outcrops at Gay’s Cove and Bath Cliffs, Barbados, in order to restudy the late Eocene microtektite layer(s) and provide new geological context. We disaggregated and processed samples into separates of microfossils, microtektites, and heavy minerals, and we present up-to-date glass geochemistry, biostratigraphic analysis, and detrital zircon U-Pb analysis. Results from the new Barbadian microtektite glass chemistry analysis (Gay’s Cove) compare well with those from other published microtektite analyses, as well as those from the correlative North American strewn field. Micropaleontology confirms a late Eocene age for the Oceanic microtektite horizon at Gay’s Cove. Using U-Pb, we dated 24 Tertiary zircon grains, probably from volcanic ash-fall events, which at Gay’s Cove yielded a preliminary, poorly defined, and incorrect depositional age for the microtektite layer (≤31.84 ± 0.85 Ma; weighted mean of only three grains). Three additional new U-Pb depositional ages (≤38.52 ± 1.0 Ma, ≤39.23 ± 0.3 Ma, ≤35.25 ± 0.82 Ma) were obtained from bottom to top in the 24 m section at Bath Cliffs. We also dated 46 Paleozoic–Proterozoic zircon grains using U-Pb and discuss whether these “old” grains represent recycled (subducted and extruded) volcanic grains or windblown silt/sand from Africa.