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natrojarosite

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Journal Article

Crystal chemistry of the natrojarosite-jarosite and natrojarosite-hydronium jarosite solid-solution series: A synthetic study with full Fe site occupancy

Laurel C. Basciano, Ronald C. Peterson
Published: 01 May 2008
American Mineralogist (2008) 93 (5-6): 853–862.
DOI: https://doi.org/10.2138/am.2008.2731
...Laurel C. Basciano; Ronald C. Peterson Abstract Members of the natrojarosite-hydronium jarosite [(Na,H 3 O)Fe 3 (SO 4 ) 2 (OH) 6 ] and jarosite-natrojarosite [(K,Na)Fe 3 (SO 4 ) 2 (OH) 6 ] solid-solution series were synthesized and investigated by Rietveld analysis of X-ray powder diffraction data...
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From schwertmannite to natrojarosite: Long-term stability and kinetic approach

Amalia Jiménez, Gregorio Marban, Ana Roza-Llera
Published: 03 January 2023
American Mineralogist (2023) 108 (1): 150–159.
DOI: https://doi.org/10.2138/am-2022-8288
... that the crystallinity of natrojarosite increases progressively with reaction time, although its cell parameters and crystallite size remain nearly constant during aging, which reveals the stability of the crystal structure of this secondary phase. Interestingly, the mechanisms governing the transformation from...
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Detection of iron substitution in natroalunite-natrojarosite solid solutions and potential implications for Mars

Thomas M. McCollom, Bethany L. Ehlmann, Alian Wang, Brian M. Hynek, Bruce Moskowitz, Thelma S. Berquó
Published: 01 May 2014
American Mineralogist (2014) 99 (5-6): 948–964.
DOI: https://doi.org/10.2138/am.2014.4617
.... Here, we evaluate the potential to use spectroscopic methods to identify minerals from the alunite group with chemical compositions intermediate between natroalunite and natrojarosite on the surface of Mars, and to remotely infer their Fe contents. X-ray diffraction and spectroscopic measurements...
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The alunite supergroup under high pressure: the case of natrojarosite, NaFe 3 (SO 4 ) 2 (OH) 6

F. Nestola, S. J. Mills, B. Periotto, L. Scandolo
Published: 01 October 2013
Mineralogical Magazine (2013) 77 (7): 3007–3017.
DOI: https://doi.org/10.1180/minmag.2013.077.7.10
...F. Nestola; S. J. Mills; B. Periotto; L. Scandolo Abstract A single crystal of natrojarosite, NaFe 3 (SO 4 ) 2 (OH) 6 , was investigated by single-crystal X-ray diffraction at high-pressure conditions (up to 8.8 GPa) using a diamond-anvil cell. The unit-cell parameters were determined at 11...
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Jarosite–butlerite intergrowths in non-stoichiometric jarosites: crystal chemistry of monoclinic natrojarosite–hydroniumjarosite phases

I. E. Grey, N. V. Y. Scarlett, P. Bordet, H. E. A. Brand
Published: 01 December 2011
Mineralogical Magazine (2011) 75 (6): 2775–2791.
DOI: https://doi.org/10.1180/minmag.2011.075.6.2775
...I. E. Grey; N. V. Y. Scarlett; P. Bordet; H. E. A. Brand Abstract Monoclinic, non-stoichiometric natrojarosite–hydroniumjarosite solid solution phases have been synthesized hydrothermally over a range of temperatures, starting compositions and reaction times, and have been characterized using...
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Quantitative microstructural characterization of natrojarosite scale formed during high-pressure acid leaching of lateritic nickel ore

Nicholas E. Timms, Jian Li, Steven M. Reddy
Published: 01 August 2009
American Mineralogist (2009) 94 (8-9): 1111–1119.
DOI: https://doi.org/10.2138/am.2009.3104
...Nicholas E. Timms; Jian Li; Steven M. Reddy Abstract The build up of scale inside autoclaves during high-pressure acid leaching of nickel laterite ore currently represents a significant industrial problem in processing plants. In this study, the crystallographic microstructure of natrojarosite...
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Natrojarosite and 'collophane' in graphite-sillimanite-schist

D. R. C. Kempe
Published: 01 May 1969
Geological Magazine (1969) 106 (3): 270–273.
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Sulfate studies IV: the jarosite—natrojarosite— hydronium jarosite solid solution series

Gerald P. Brophy, Michael F. Sheridan
Published: 01 October 1965
American Mineralogist (1965) 50 (10): 1595–1607.
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Journal Article

Natrojarosite from near the Montana-Wyoming line

Richard S. Mitchell, William F. Giannini
Published: 01 December 1958
American Mineralogist (1958) 43 (11-12): 1205–1210.
...Richard S. Mitchell; William F. Giannini Abstract The purpose of this paper is to report an occurrence of natrojarosite, NaFe 3 (SO 4 ) 2 (OH) 6 , near the Montana-Wyoming line. The senior writer first noticed this material in August of 1954, but was not able to study it adequately until more...
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BSE images of Js-SB-35. ( a ) Pseudocubic <span class="search-highlight">natrojarosite</span> crystals. ( b ) Tab...

BSE images of Js-SB-35. ( a ) Pseudocubic natrojarosite crystals. ( b ) Tab...

Published: 01 March 2023
Figure 9. BSE images of Js-SB-35. ( a ) Pseudocubic natrojarosite crystals. ( b ) Tabular, striated gypsum intermixed with pseudocubic natrojarosite. ( c ) A rounded, zircon crystal surrounded by natrojarosite (light gray) and quartz (darker gray and rounded) crystals ( d ) A phosphate mineral
Image
BSE images: ( a ) striated crystals of gypsum; microcrystals of natrojarosi...

BSE images: ( a ) striated crystals of gypsum; microcrystals of natrojarosi...

Published: 01 October 2014
F ig . 3. BSE images: ( a ) striated crystals of gypsum; microcrystals of natrojarosite and several paler flat halite grains are scattered around the crystals of gypsum; ( b ) skeletal crystals of gypsum among spherical aggregates of magnesiocopiapite; ( c ) dissolution of gypsum crystals along
Image
SEM images of iron hydroxysulfates. ( a ) The surface of schwertmannite is ...

SEM images of iron hydroxysulfates. ( a ) The surface of schwertmannite is ...

Published: 03 January 2023
Figure 4. SEM images of iron hydroxysulfates. ( a ) The surface of schwertmannite is composed by aggregate of particles. ( b ) Natrojarosite crystals. ( c ) Rhombohedral crystals of natrojarosite.
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( a ) Linear fitting of the time (ln t = 0.95) for a 95% fraction of trans...

( a ) Linear fitting of the time (ln t = 0.95) for a 95% fraction of trans...

Published: 03 January 2023
Figure 9. ( a ) Linear fitting of the time (ln t = 0.95) for a 95% fraction of transformed natrojarosite vs. the reciprocal of temperature. ( b ) TTT graph corresponding to a fraction Y = 0.95 of the transformed natrojarosite.
Image
Partial PXRD pattern as a function of temperature for in situ decomposition...

Partial PXRD pattern as a function of temperature for in situ decomposition...

Published: 01 March 2023
Figure 5. Partial PXRD pattern as a function of temperature for in situ decomposition of Js-SB-35A natrojarosite. The transformation from monoclinic (M) to rhombohedral (R) natrojarosite is indicated. A peak associated with quartz is noted. (Color online.)
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Schematic diagram of <span class="search-highlight">natrojarosite</span> scale accumulation. ( a ) Profile of sca...

Schematic diagram of natrojarosite scale accumulation. ( a ) Profile of sca...

Published: 01 August 2009
F igure 8. Schematic diagram of natrojarosite scale accumulation. ( a ) Profile of scale showing elongate natrojarosite grains with compositional banding. Minor phases primarily located along grain boundaries. ( b ) Detail of a showing subgrains within natrojarosite grains. ( c ) Lower
Image
EBSD image of the thin section of Js-SB-35A highlighting regions that index...

EBSD image of the thin section of Js-SB-35A highlighting regions that index...

Published: 01 March 2023
Figure 10. EBSD image of the thin section of Js-SB-35A highlighting regions that index as monoclinic natrojarosite (M; purple), rhombohedral natrojarosite (R; blue), or can be indexed using either a monoclinic or rhombohedral model (I; mottled blue and purple). Black regions correspond
Image
X-ray diffraction patterns for Fe-sulfates: ( a ) jarosite, ( b ) jarosite ...

X-ray diffraction patterns for Fe-sulfates: ( a ) jarosite, ( b ) jarosite ...

Published: 01 August 2014
Figure 2 X-ray diffraction patterns for Fe-sulfates: ( a ) jarosite, ( b ) jarosite + natrojarosite, ( c ) natrojarosite, ( d ) szomolnokite, ( e ) rhomboclase, and ( f ) melanterite. The intensity of each pattern has been normalized to 1 and offset by 1 for clarity.
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Powder XRD patterns of the same sample of monoclinic <span class="search-highlight">Natrojarosite</span> taken on...

Powder XRD patterns of the same sample of monoclinic Natrojarosite taken on...

Published: 01 November 2018
Figure 9. Powder XRD patterns of the same sample of monoclinic Natrojarosite taken on a laboratory instrument (black) and at the PD beamline at the Australian Synchrotron (grey). The inset is an enlarged section of the patterns to highlight the difference in quality. The data have been converted
Image
Chinleite-(Y) with <span class="search-highlight">natrojarosite</span> (yellow) on quartz; field of view: 0.5 mm ...

Chinleite-(Y) with natrojarosite (yellow) on quartz; field of view: 0.5 mm ...

Published: 01 August 2017
Fig. 2. Chinleite-(Y) with natrojarosite (yellow) on quartz; field of view: 0.5 mm across.
Journal Article

The occurrence of monoclinic jarosite in natural environments

Anne J. Whitworth, Helen E.A. Brand, Sasha Wilson, Ian E. Grey, Natasha R. Stephen, Yesim Gozukara, Andrew J. Frierdich
Published: 01 March 2023
American Mineralogist (2023) 108 (3): 584–594.
DOI: https://doi.org/10.2138/am-2022-8276
...Figure 9. BSE images of Js-SB-35. ( a ) Pseudocubic natrojarosite crystals. ( b ) Tabular, striated gypsum intermixed with pseudocubic natrojarosite. ( c ) A rounded, zircon crystal surrounded by natrojarosite (light gray) and quartz (darker gray and rounded) crystals ( d ) A phosphate mineral...
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