Quantitative compositional mapping of mineral phases by electron probe micro-analyser
Published:April 17, 2019
Pierre Lanari, Alice Vho, Thomas Bovay, Laura Airaghi, Stephen Centrella, 2019. "Quantitative compositional mapping of mineral phases by electron probe micro-analyser", Metamorphic Geology: Microscale to Mountain Belts, Silvio Ferrero, Pierre Lanari, Philippe Goncalves, Eugene G. Grosch
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Compositional mapping has greatly impacted mineralogical and petrological studies over the past half-century with increasing use of the electron probe micro-analyser. Many technical and analytical developments have benefited from the synergies of physicists and geologists and they have greatly contributed to the success of this analytical technique. Large-area compositional mapping has become routine practice in many laboratories worldwide, improving our ability to measure the compositional variability of minerals in natural geological samples and reducing the operator bias as to where to locate single spot analyses. This chapter aims to provide an overview of existing quantitative techniques for the evaluation of rock and mineral compositions and to present various examples of applications. A new advanced method for compositional map standardization that relies on internal standards and accurately corrects the X-ray intensities for continuum background is also presented. This technique has been implemented into the computer software XMapTools. The improved workflow defines the appropriate practice of accurate standardization and provides data-reporting standards to help improve petrological interpretations.
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Metamorphic Geology: Microscale to Mountain Belts
CONTAINS OPEN ACCESS
In Earth evolution, mountain belts are the loci of crustal growth, reworking and recycling. These crustal-scale processes are unravelled through microscale investigations of textures and mineral assemblages of metamorphic rocks. Multiple episodes of metamorphism, re-equilibration and deformation, however, generally produce a complex and tightly interwoven pattern of microstructures and assemblages. Over the last two decades, the combination of advanced computing and technological capabilities with new concepts has provided a vast array of novel petrological tools and high-resolution/high-sensitivity techniques for microanalysis and imaging. Such novel approaches are proving fundamental to untangling the enigma represented by metamorphism with an unprecedented level of detail and confidence. As a result, the first decade and a half of this century has already seen the tumultuous development of new research avenues in metamorphic petrology. This book aims to provide a timely overview of the state of the art of this field, of newly developed petrological techniques, future advancements and significant new case studies.